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Standard operating procedure for soil total nitrogen - Dumas dry combustion method










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    Booklet
    Standard operating procedure for soil nitrogen - Kjeldahl method 2021
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    This standard operating procedure (SOP) describes, in general terms, the quantification of the Kjeldahl nitrogen(KjN) content in soil samples. The advantages of this method are based on its robustness, low initial cost of the equipment and extensive application. However, there are disadvantages in using this method compared to others, for example, the use of potentially hazardous reagents that require consideration for safe operation are utilized, alongside the generation of hazardous waste and on-going cost of consumables, which can be mitigated via modified protocols that use lower quantities of reagents. Another limitation of this method is that it measures organic N and mineral N in the form of ammonium cation (NH4+), therefore, to measure the total N, the mineral N in the form of NO3- must be measured separately
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    Standard operating procedure for soil available phosphorus - Olsen method 2021
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    This procedure is suitable for calcareous, alkaline, neutral, and slightly acidic soils containing CaPO4, since the calcium concentration in the solution is suppressed by the precipitation of CaCO3, increasing PO4 concentration in solution. Neutral and slightly acid soils (pH 6.0 to 7.0) may contain both Ca- and Al-phosphates. The NaHCO3 extractant can remove Ca-phosphates and phosphate adsorbed on the surface of calcium and magnesium carbonates along with Al-phosphates and is considered the most suitable extractant for these soils.
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    Brochure, flyer, fact-sheet
    Standard operating procedure for quasi total elements in soil by acid digestion, including heavy metals 2023
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    This method is applicable to the determination of trace element metals (MTE) as well as metalloids in soils by acid digestion using aqua regia.

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