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Manual of Standard Operating Procedures for Selected Chemical Residue and Contaminant Analysis

Year of publication 2021

Place of publication Vienna, Austria ;

Pages 324 p.

Author FAO, IAEA

Publisher FAO, IAEA ;

Product type Book (stand-alone)

ISBN 978-92-5-134812-3

Edition 1

To cite or share https://doi.org/10.4060/cb6191en

Synopsis (short abstract) Food safety is an important global public health and trade matter, with chemical hazards occupying centre stage due to associated acute and chronic health outcomes. There is also an increasing need to address antimicrobial resistance concerns. While food remains a major vehicle for exposure to these hazards, related matrices cannot be ignored. Animal feed for instance may contain drug or pesticide residues as well as mycotoxins that could carry-over to food either as parent compounds or their metabolites of toxicological relevance. Contaminated water is also another medium of potential exposure to food hazards. A concerted effort is required to address the need for a safe food supply and one critical stakeholder is the testing laboratory. While this requires trained and capable analysts as well as reliable instrumentation, analytical methods are a major need. Development and validation – to ensure fitness of purpose – and availability of these methods is a necessity. This manual, consisting of several Standard Operating Procedures (SOPs), presents another opportunity for laboratories to address gaps in analytical methods and/or expand their options. The manual contains techniques for analyzing certain mycotoxins such as aflatoxins, fumonisin and ochratoxin in matrices that include milk, edible vegetable oil and animal feed etc. A range of veterinary drug residues including permitted and prohibited substances in animal matrices including fish, are also addressed. Several pesticide residues in cereals, fruits and vegetables are also covered. A couple of methods for analysis of selected metals are also presented.

Cite this content as:

FAO and IAEA. 2021.  Manual of Standard Operating Procedures for Selected Chemical Residue and Contaminant Analysis. Vienna.

https://doi.org/10.4060/cb6191en

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    Carryover of veterinary drugs in feed can occur during feed processing, handling, transportation, delivery or in feeding animals on-farm. The risk of unavoidable and unintentional veterinary drug residues from feed carryover and/or transfer from feed to food of animal origin is unacceptable when it causes adverse health effects in target and/or non-target animals and/or humans consuming food originating from these animals. If carryover is not properly managed, contaminated feed can directly harm species that are sensitive to the unintended veterinary drug they consume, and /or can result in residues in food of animal origin such as meat, milk and eggs that render them unsafe for human consumption. Even if residues are not a safety hazard, they can pose regulatory and global trade issue as countries/markets may enforce a “zero” tolerance for residues when appropriate maximum residue limits have not been established. Upon request of the Codex Committee on Residues of Veterinary Drugs in Foods (CCRVDF), FAO and WHO convened an Expert Meeting to review the causes of veterinary drug carryover in animal feed and the transfer from feed to food, as well as the known risks to human health and international trade, and suggest appropriate risk management strategies. This report shows the results of the expert discussions, conclusions and recommendations.
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